FMOC-L-苯丙氨酸五氟苯酯合成路线 （共 14 条）
反应条件
pyridine in tetrahydrofuran T=4°C;
参考文献
Jacobsen, Mogens Havsteen; Buchardt, Ole; Engdahl, Tom; Holm, Arne
Tetrahedron Letters, 1991 , vol. 32, # 43 p. 6199 - 6202
反应条件
benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=20°C; Esterification;
参考文献
Pudhom, Khanitha; Vilaivan, Tirayut
Tetrahedron Letters, 1999 , vol. 40, # 32 p. 5939 - 5942
反应条件
dicyclohexyl-carbodiimide in ethyl acetate 0 deg C, 1 h; r.t., 1 h;
参考文献
Kisfaludy, Lajos; Schoen, Istvan
Synthesis, 1983 , # 4 p. 325 - 327
反应条件
pyridine in N,N-dimethyl-formamide 0.75 h; Ambient temperature;
参考文献
Green, Michael; Berman, Judd
Tetrahedron Letters, 1990 , vol. 31, # 41 p. 5851 - 5852
参考文献
Il'ina, A. V.; Davidovich, Yu. A.; Rogozhin, S. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 12 p. 2539 - 2541
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 12 p. 2816 - 2818
反应条件
1: 89 percent / pyridine, SOCl2 / diethyl ether / 0.5 h / 0 - 20 °C 2: 93 percent / pyridine / 20 °C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, # 12 p. 2539 - 2541
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2816 - 2818
反应条件
1: SOCl2, pyridine / CH2Cl2 / Heating 2: 88 percent / pyridine / tetrahydrofuran / 4 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 43 p. 6199 - 6202
反应条件
1: 86 percent / NaHCO3 / H2O; acetone / Ambient temperature 2: dicyclohexylcarbodiimide / ethyl acetate / 2 h / 0 °C View Scheme
参考文献
Synthesis, , # 4 p. 303 - 305
反应条件
1: 86 percent / NaHCO3 / H2O; acetone / Ambient temperature 2: dicyclohexylcarbodiimide / ethyl acetate / 2 h / 0 °C View Scheme
参考文献
Synthesis, , # 4 p. 303 - 305
反应条件
solid phase synthesis; Multistep reaction;
参考文献
Funakoshi, Susumu; Murayama, Eigoro; Guo, Lili; Fujii, Nobutaka; Yajima, Haruaki
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 11B p. 2791 - 2800
