4-氯-2-乙炔基-1-硝基苯合成路线 （共 6 条）
反应条件
potassium carbonate in methanol
T=20°C; 4 h;
参考文献
STATE OF OREGON ACTING BY AND THROUGH THE STATE BOARD OF HIGHER EDUCATION ON BEHALF OF OREGON STATE UNIVERSITY
Patent: WO2008/156656 A2, 2008 ;
Location in patent: Page/Page column 44; 182 ;
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 2 h / 50 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride; water / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
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参考文献
Jadhav, Appaso Mahadev; Bhunia, Sabyasachi; Liao, Hsin-Yi; Liu, Rai-Shung
Journal of the American Chemical Society, 2011 , vol. 133, # 6 p. 1769 - 1771
参考文献
Schofield; Swain
Journal of the Chemical Society, 1949 , p. 2393,2396
反应条件
1: pyridine; piperidine
2: acetic acid; bromine / 95 °C
3: aq.-ethanolic NaOH-solution
4: water
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参考文献
Schofield; Swain
Journal of the Chemical Society, 1949 , p. 2393,2396
反应条件
1: acetic acid; bromine / 95 °C
2: aq.-ethanolic NaOH-solution
3: water
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参考文献
Schofield; Swain
Journal of the Chemical Society, 1949 , p. 2393,2396
反应条件
1: aq.-ethanolic NaOH-solution
2: water
View Scheme
参考文献
Schofield; Swain
Journal of the Chemical Society, 1949 , p. 2393,2396
