(R)-3-丁烯-1,2-二醇合成路线 (共 21 条)
反应条件
hydrogen; Wilkinson's catalyst in benzene Yield given. Title compound not separated from byproducts;
参考文献
Howes, David A.; Brookes, Michael H.; Coates, Dinah; Golding, Bernard T.; Hudson, Alan T.
Journal of Chemical Research, Miniprint, 1983 , # 1 p. 217 - 228
反应条件
horse liver alcohol dehydrogenase in water T=37°C; Oxidation; pH=7.4; 0.05 h; Enzymatic reaction; Enzyme kineticsProduct distribution;
参考文献
Kemper, Raymond A.; Elfarra, Adnan A.
Chemical Research in Toxicology, 1996 , vol. 9, # 7 p. 1127 - 1134
反应条件
hydrogen; platinum(IV) oxide in methanol 16 h; Yield given;
参考文献
Howes, David A.; Brookes, Michael H.; Coates, Dinah; Golding, Bernard T.; Hudson, Alan T.
Journal of Chemical Research, Miniprint, 1983 , # 1 p. 217 - 228
反应条件
hydrogen; Wilkinson's catalyst in benzene Yield given. Title compound not separated from byproducts;
参考文献
Howes, David A.; Brookes, Michael H.; Coates, Dinah; Golding, Bernard T.; Hudson, Alan T.
Journal of Chemical Research, Miniprint, 1983 , # 1 p. 217 - 228
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in tetrahydrofuran T=0 - 20°C; Inert atmosphere; regioselective reaction;
参考文献
Stambasky, Jan; Kapras, Votech; Stefko, Martin; Kysilka, Ondrej; Hocek, Michal; Malkov, Andrei V.; Kocovsky, Pavel
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7781 - 7803
反应条件
in pyridine T=0 - 4°C; Title compound not separated from byproducts;
参考文献
Richardson, Kevan A.; Peters, Melanie M. C. G.; Megens, Rene H. J. J. J.; Van Elburg, Paul A.; Golding, Bernard T.; Boogaard, Peter J.; Watson, William P.; Van Sittert, Nico J.
Chemical Research in Toxicology, 1998 , vol. 11, # 12 p. 1543 - 1555
反应条件
tert.-butylhydroperoxide; sodium hydride in N,N-dimethyl-formamide; mineral oil
T=0 - 20°C; enantioselective reaction;
参考文献
Kaviani-Joupari, Makan; Schramm, Michael P.
Tetrahedron Letters, 2013 , vol. 54, # 37 p. 5014 - 5017
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran
T=0 - 20°C; 72 h;
参考文献
Ready; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 11 p. 2687 - 2688
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C; 72 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315