N-[1-(1H-苯并三唑-1-基)-2,2-二甲基丙基]-3,4-二甲氧基苯乙酰胺合成路线 （共 4 条）
反应条件
caesium carbonate in acetonitrile T=23°C; 10 h;
参考文献
Perez-Medrano, Arturo; Donnelly-Roberts, Diana L.; Honore, Prisca; Hsieh, Gin C.; Namovic, Marian T.; Peddi, Sridhar; Shuai, Qi; Wang, Ying; Faltynek, Connie R.; Jarvis, Michael F.; Carroll, William A.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 10 p. 3366 - 3376
反应条件
toluene-4-sulfonic acid in toluene
10 h; Reflux;
参考文献
Perez-Medrano, Arturo; Donnelly-Roberts, Diana L.; Honore, Prisca; Hsieh, Gin C.; Namovic, Marian T.; Peddi, Sridhar; Shuai, Qi; Wang, Ying; Faltynek, Connie R.; Jarvis, Michael F.; Carroll, William A.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 10 p. 3366 - 3376
反应条件
1.1: thionyl chloride / dichloromethane
2.1: ammonia / tetrahydrofuran
3.1: toluene-4-sulfonic acid / toluene / Reflux
3.2: 60 - 65 °C
View Scheme
参考文献
Gudaparthi, Vijayalakshmi; Bharathi; Panda, Jagadeesh
Asian Journal of Chemistry, 2010 , vol. 22, # 7 p. 5323 - 5330
反应条件
1.1: ammonia / tetrahydrofuran
2.1: toluene-4-sulfonic acid / toluene / Reflux
2.2: 60 - 65 °C
View Scheme
参考文献
Gudaparthi, Vijayalakshmi; Bharathi; Panda, Jagadeesh
Asian Journal of Chemistry, 2010 , vol. 22, # 7 p. 5323 - 5330
