7-甲氧基-3,4-二氢-1-萘基乙腈合成路线 (共 4 条)
反应条件
hexane carboxylic acid; benzylamine in toluene Heating / reflux; Product distribution / selectivity;
参考文献
Souvie, Jean-Claude; Gonzalez Blanco, Isaac; Thominot, Gilles; Chapuis, Genevieve; Horvath, Stephane; Damien, Gerard
Patent: US2005/182276 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: hydrogen; ammonia / Raney nickel / ethanol; water / 3 h / 40 °C / Autoclave vessel 2: ethanol / 0.5 h / 0 - 5 °C 3: sulfur / 0.5 h / 180 °C View Scheme
参考文献
CADILA HEALTHCARE LIMITED; DWIVEDI, Shri Prakash Dhar; PRASAD, Ashok; SHAH, Niraj Shyamlal; PATEL, Mayur Ramnikbhai
Patent: WO2014/72998 A1, 2014 ;
反应条件
1: hydrogen; ammonia / Raney nickel / ethanol; water / 3 h / 40 °C / Autoclave vessel 2: hydrogenchloride / ethyl acetate / 0.5 h / 0 - 5 °C 3: sulfur / 0.5 h / 180 - 185 °C View Scheme
反应条件
ethylene,methyl methacrylate; palladium on activated carbon in toluene Heating / reflux;
参考文献
Souvie, Jean-Claude; Gonzalez Blanco, Isaac; Thominot, Gilles; Chapuis, Genevieve; Horvath, Stephane; Damien, Gerard
Patent: US2005/182276 A1, 2005 ;
Location in patent: Page/Page column 6 ;