5-溴-2,3-二氢-1H-茚-2-醇乙酸酯合成路线 （共 5 条）
反应条件
1: With sodium hydroxide in methanol T=0 - 25°C; 2: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile T=20°C; Further stages.;
参考文献
Tetrahedron Asymmetry, , vol. 18, # 6 p. 717 - 723
反应条件
sodium hydroxide in methanol; water T=25°C; 15 h;
参考文献
Goeksu, Sueleyman; Secen, Hasan
Tetrahedron, 2005 , vol. 61, # 28 p. 6801 - 6807
反应条件
1: 90 percent / NaOH / methanol; H2O / 15 h / 25 °C 2: 84 percent / PPh3; DEAD; HN3 / tetrahydrofuran / 12.5 h / 0 - 25 °C 3: 80 percent / CuSO4*5H2O; NaBH4 / methanol / 3 h / 25 °C View Scheme
参考文献
Goeksu, Sueleyman; Secen, Hasan
Tetrahedron, 2005 , vol. 61, # 28 p. 6801 - 6807
反应条件
N-bromosuccinmide in acetonitrile
T=25°C; 168 h;
参考文献
Goeksu, Sueleyman; Secen, Hasan
Tetrahedron, 2005 , vol. 61, # 28 p. 6801 - 6807
反应条件
1: 100 percent / 16 h / 25 °C
2: 83 percent / N-bromosuccinimide / acetonitrile / 168 h / 25 °C
View Scheme
参考文献
Goeksu, Sueleyman; Secen, Hasan
Tetrahedron, 2005 , vol. 61, # 28 p. 6801 - 6807
