(S)-4-苯基-2-恶唑烷酮合成路线 （共 47 条）
反应条件
(R)-2-phenyl-1,2-dihydroimidazo[1,2-a]quinoline; N-ethyl-N,N-diisopropylamine in chloroform T=0°C; 3.5 h; Title compound not separated from byproducts;
参考文献
Birman, Vladimir B.; Jiang, Hui; Li, Ximin; Guo, Lei; Uffman, Eric W.
Journal of the American Chemical Society, 2006 , vol. 128, # 20 p. 6536 - 6537
反应条件
(R)-2-phenyl-1,2-dihydroimidazo[1,2-a]quinoline; N-ethyl-N,N-diisopropylamine in chloroform T=0°C; 3.5 h; Title compound not separated from byproducts;
参考文献
Birman, Vladimir B.; Jiang, Hui; Li, Ximin; Guo, Lei; Uffman, Eric W.
Journal of the American Chemical Society, 2006 , vol. 128, # 20 p. 6536 - 6537
反应条件
[bis(acetoxy)iodo]benzene; silver nitrate; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in acetonitrile
T=82°C;
参考文献
Cui, Yong; He, Chuan
Angewandte Chemie - International Edition, 2004 , vol. 43, # 32 p. 4210 - 4212
反应条件
Rh2(triphenylacetate)4; potassium carbonate in dichloromethane
T=25°C; 6 h;
参考文献
Huard, Kim; Lebel, Helene
Chemistry - A European Journal, 2008 , vol. 14, # 20 p. 6222 - 6230
反应条件
4-(N,N-dimethlyamino)pyridine; 4-methoxy-phenol in dichloromethane
T=120°C; P=26777.7 Torr; 48 h;
参考文献
Shen, Yu-Mei; Duan, Wei-Liang; Shi, Min
European Journal of Organic Chemistry, 2004 , # 14 p. 3080 - 3089
反应条件
lithium bromide in 1-methyl-pyrrolidin-2-one
T=100°C; P=760 Torr; 24 h;
参考文献
Sudo, Atsushi; Morioka, Yosuke; Koizumi, Eri; Sanda, Fumio; Endo, Takeshi
Tetrahedron Letters, 2003 , vol. 44, # 43 p. 7889 - 7891
反应条件
boron trifluoride diethyl etherate; benzenetellurinyl trifluoroacetate in 1,2-dichloro-ethane
24 h; Heating;
参考文献
Hu, Nan X.; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio
Journal of the Chemical Society, Chemical Communications, 1987 , # 19 p. 1447 - 1448
反应条件
1: With sodium hydride in tetrahydrofuran
T=-78°C; 0.5 h;
2: With trimethylphosphane in tetrahydrofuran
T=-78 - 20°C;
参考文献
Ariza, Xavier; Pineda, Oriol; Urpi, Felix; Vilarrasa, Jaume
Tetrahedron Letters, 2001 , vol. 42, # 30 p. 4995 - 4999
反应条件
hydrogen; palladium on activated charcoal in acetic acid
参考文献
Rodehorst,R.M.; Koch,T.H.
Journal of the American Chemical Society, 1975 , vol. 97, p. 7298 - 7304
反应条件
1: benzene / Irradiation
2: H2 / Pd-C / acetic acid
View Scheme
参考文献
Rodehorst,R.M.; Koch,T.H.
Journal of the American Chemical Society, 1975 , vol. 97, p. 7298 - 7304
