(1-甲基-4-苯基-1,2,3,6-四氢-3-吡啶基)甲醇合成路线 （共 6 条）
反应条件
potassium permanganate in acetonitrile T=20°C; 1.5 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 39, # 4 p. 471 - 477
反应条件
manganese(IV) oxide; sodium hydroxide in benzene
T=20 - 40°C; 1.5 h;
参考文献
Soldatenkov; Temesgen; Polyanskii; Soldatova; Kolyadina; Golovtsov; Sergeeva
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 4 p. 471 - 477
反应条件
manganese(IV) oxide in benzene
T=20°C; 2 h;
参考文献
Soldatenkov; Temesgen; Polyanskii; Soldatova; Kolyadina; Golovtsov; Sergeeva
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 4 p. 471 - 477
反应条件
formic acid
12 h; Heating;
参考文献
Sohar, Pal; Lazar, Janos; Bernath, Gabor
Chemische Berichte, 1985 , vol. 118, # 2 p. 551 - 559
反应条件
sulfuric acid; water
Erwaermen des Reaktionsgemisches mit 1-Methyl-4-phenyl-1,2,3,6-tetrahydro-pyridin oder mit (+-)-3,6-Dimethyl-6-phenyl-tetrahydro-<1,3>oxazin.;
参考文献
Rohm and Haas Co.
Patent: US2748140 , 1954 ;
反应条件
1: 1.) NH4Cl, 2.) conc. HCl / 1.) MeOH, 40 deg C, 20 h, 2.) 100 deg C
2: 89 percent / HCOOH / 12 h / Heating
View Scheme
参考文献
Sohar, Pal; Lazar, Janos; Bernath, Gabor
Chemische Berichte, 1985 , vol. 118, # 2 p. 551 - 559
