2-苯基-4-(对二甲氨基苯基)-吡咯合成路线 （共 3 条）
反应条件
1.1: KOH / methanol; tetrahydrofuran / 1 h / 20 °C
1.2: H2SO4 / tetrahydrofuran / 1 h / 20 °C
2.1: 0.34 g / AcOH; NH4OAc / 1 h / 100 °C
View Scheme
参考文献
Hall, Michael J.; McDonnell, Shane O.; Killoran, John; O'Shea, Donal F.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5571 - 5578
反应条件
1.1: 76 percent / KOH / ethanol; H2O
2.1: 87 percent / Et2NH / methanol / 16 h / Heating
3.1: KOH / methanol; tetrahydrofuran / 1 h / 20 °C
3.2: H2SO4 / tetrahydrofuran / 1 h / 20 °C
4.1: 0.34 g / AcOH; NH4OAc / 1 h / 100 °C
View Scheme
参考文献
Hall, Michael J.; McDonnell, Shane O.; Killoran, John; O'Shea, Donal F.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5571 - 5578
反应条件
1.1: 76 percent / KOH / ethanol; H2O
2.1: 87 percent / Et2NH / methanol / 16 h / Heating
3.1: KOH / methanol; tetrahydrofuran / 1 h / 20 °C
3.2: H2SO4 / tetrahydrofuran / 1 h / 20 °C
4.1: 0.34 g / AcOH; NH4OAc / 1 h / 100 °C
View Scheme
参考文献
Hall, Michael J.; McDonnell, Shane O.; Killoran, John; O'Shea, Donal F.
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5571 - 5578
