[双-(2-羟基-乙基)-氨基]- 乙腈合成路线 (共 4 条)
反应条件
1: With C46H178O41Si42; titanium (IV) isopropoxide in toluene T=60°C; 24 h; Inert atmosphere; 2: With water; sodium hydroxide in toluene T=20°C; 4 h; Inert atmosphere;
参考文献
Laval, Stephane; Dayoub, Wissam; Pehlivan, Leyla; Metay, Estelle; Favre-Reguillon, Alain; Delbrayelle, Dominique; Mignani, Gerard; Lemaire, Marc
Tetrahedron, 2014 , vol. 70, # 4 p. 975 - 983
反应条件
triethylamine in methanol; dichloromethane
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5210271 A1, 1993 ;
反应条件
potassium carbonate in tetrahydrofuran
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5210271 A1, 1993 ;
反应条件
T=10 - 15°C; zuletzt bei 60grad;
参考文献
I.G.Farbenind.
Patent: DE564787 , 1931 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 1470
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I.G.Farbenind.
Patent: US1972465 , 1932 ;