3-溴-4,5-二氢-5-苯基异噁唑合成路线 （共 7 条）
反应条件
potassium hydrogencarbonate in water; N,N-dimethyl-formamide T=-10 - 20°C; 2 h; Inert atmosphere; regioselective reaction;
参考文献
Girardin, Melina; Alsabeh, Pamela G.; Lauzon, Sophie; Dolman, Sarah J.; Ouellet, Stephane G.; Hughes, Greg
Organic Letters, 2009 , vol. 11, # 5 p. 1159 - 1162
反应条件
NOCl*2SO3 in dichloromethane T=0°C; 1 h;
参考文献
Bondarenko; Gavrilova; Saginova; Zyk; Zefirov
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 2 p. 218 - 225
反应条件
sulfur dioxide; nitrosyl chloride in dichloromethane T=-20°C; 18 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 45, # 2 p. 218 - 225
反应条件
sodium hydrogencarbonate in ethyl acetate Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 46, # 6 p. 1975 - 1986
反应条件
sodium nitrite in chloroform; trifluoroacetic acid T=-5°C; 0.5 h; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 3 p. 246 - 250
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 20, # 3 p. 309 - 313
反应条件
ethyl mercaptan sodium salt in methanol T=0 - 20°C; 0.666667 h;
参考文献
Min Hyo Seo; Youn Young Lee; Yang Mo Goo
Synthetic Communications, 1994 , vol. 24, # 10 p. 1433 - 1439
反应条件
1: 100 percent / five fold excess of lihium methoxide
2: 76 percent / H2, B(OH)3 / Raney-Ni
View Scheme
参考文献
Caldilora, P.; Ciancaglione, M.; De Amici, M.; De Micheli, C.
Tetrahedron Letters, 1986 , vol. 27, # 38 p. 4647 - 4650
