1H-苯并三唑-1-甲酸甲酯合成路线 (共 8 条)
反应条件
T=120°C; Title compound not separated from byproducts;
参考文献
Journal of Physical Organic Chemistry, , vol. 6, # 10 p. 567 - 573
反应条件
T=120°C; Title compound not separated from byproducts;
参考文献
Krollpfeiffer et al.
Chemische Berichte, 1938 , vol. 71, p. 596,602
反应条件
N,N,N',N,-tetramethylethylenediamine in N,N-dimethyl-formamide
T=95°C;
参考文献
Zhao, Sheng-Yin; Zhang, Hai-Quan; Zhang, Deng-Qing; Shao, Zhi-Yu
Synthetic Communications, 2012 , vol. 42, # 1 p. 128 - 135
反应条件
1: 1-N-(1-ferrocenyl-1-methyl)ethylbenzotriazole With n-butyllithium in tetrahydrofuran; hexane
T=-70 - 20°C; Inert atmosphere;
2: methyl chloroformate in tetrahydrofuran; hexane
Inert atmosphere;
3: water in thiophene; hexane
参考文献
Moiseev; Cherevatskaya; Verbitskaya; Glukhov; Peregudov; Kalinin
Russian Chemical Bulletin, 2012 , vol. 61, # 10 p. 1933 - 1942
Izv. Akad. Nauk, Ser. Khim., 2012 , # 10 p. 1918 - 1927,10
反应条件
Ambient temperature;
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
反应条件
1: 50 percent / CH2Cl2; toluene / 1 h / Ambient temperature
2: 90 percent / Ambient temperature
View Scheme
参考文献
Katritzky, Alan R.; Zhang, Gui-Fen; Fan, Wei-Qiang; Wu, Jing; Pernak, Juliusz
Journal of Physical Organic Chemistry, 1993 , vol. 6, # 10 p. 567 - 573
参考文献
Krollpfeiffer et al.
Chemische Berichte, 1938 , vol. 71, p. 596,602
参考文献
Kalcic, Igor; Zovko, Marijana; Takac, Milena Jadrijevic-Mladar; Zorc, Branka; Butula, Ivan
Croatica Chemica Acta, 2003 , vol. 76, # 3 p. 217 - 228