methanol in dichloromethane; pentane
under N2; soln. of B complex in CH2Cl2 cooled to 0 °C, slowly added to cold (-10 °C) mixt. of glycol and pentane, stirred for 0.5h at -10 °C, added MeOH, stirred for 10 min; upper layer sepd., lower layer extd. with cold (0 °C) pentane, combined ext. evapd. in vac., distd.;
参考文献
Brown, Herbert C.; Bhat N. G.; Somayaji, Vishwanatha
Organometallics, 1983 , vol. 2, p. 1311 - 1316
styrene; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,2-dichloro-ethane
参考文献
Murata, Miki; Kawakita, Koji; Asana, Taichi; Watanabe, Shinji; Masuda, Yuzuru
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 825 - 829
