[RhCl(η2:η2-cycloocta-1,5-diene)]2 in toluene
pinacolborane and vinylarene were added to a mixt. of Rh-complex in toluene under Ar, the mixt. was stirred at room temp. for 4 h; diluted with toluene, washed with water, dried over MgSO4, evapd., distilled with Kugelrohr or chromy. on silica gel;
参考文献
Murata, Miki; Kawakita, Koji; Asana, Taichi; Watanabe, Shinji; Masuda, Yuzuru
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 825 - 829
[RhCl(η2:η2-cycloocta-1,5-diene)]2 in toluene
pinacolborane and vinylarene were added to a mixt. of Rh-complex in toluene under Ar, the mixt. was stirred at room temp. for 4 h; diluted with toluene, washed with water, dried over MgSO4, evapd., distilled with Kugelrohr or chromy. on silica gel;
参考文献
Murata, Miki; Kawakita, Koji; Asana, Taichi; Watanabe, Shinji; Masuda, Yuzuru
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 825 - 829
