1,3-苯并二氧戊环-4,7-二酮合成路线 （共 5 条）
反应条件
1: hydrogen / Pd-C / tetrahydrofuran
2: 64 percent / ceric ammonium nitrate / acetonitrile / 0.08 h
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
ammonium cerium(IV) nitrate in acetonitrile
0.0833333 h;
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: 100 percent / K2CO3 / dimethylformamide / 60 °C
2: 14 percent / POCl3 / chlorobenzene / 1.) -5 deg C, 2.) -5 deg C to room temperature
3: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
4: hydrogen / Pd-C / tetrahydrofuran
5: 64 percent / ceric ammonium nitrate / acetonitrile / 0.08 h
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: 14 percent / POCl3 / chlorobenzene / 1.) -5 deg C, 2.) -5 deg C to room temperature
2: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
3: hydrogen / Pd-C / tetrahydrofuran
4: 64 percent / ceric ammonium nitrate / acetonitrile / 0.08 h
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
2: hydrogen / Pd-C / tetrahydrofuran
3: 64 percent / ceric ammonium nitrate / acetonitrile / 0.08 h
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
