1,3-苯并二氧戊环-4,7-二醇合成路线 （共 8 条）
反应条件
sodium hydroxide; dipotassium peroxodisulfate
Erwaermen des nach Ansaeuern geloesten Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: 14 percent / POCl3 / chlorobenzene / 1.) -5 deg C, 2.) -5 deg C to room temperature
2: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
3: hydrogen / Pd-C / tetrahydrofuran
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: 97 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
2: hydrogen / Pd-C / tetrahydrofuran
View Scheme
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
反应条件
1: quinoline; copper oxide-chromium oxide catalyst
2: aq. NaOH solution; aqueous potassium peroxo disulfate solution / Erwaermen des nach Ansaeuern geloesten Reaktionsprodukts mit wss. Salzsaeure
View Scheme
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
1: acetone; aq. NaOH solution / unter Ausschluss von Luft
2: quinoline; copper oxide-chromium oxide catalyst
3: aq. NaOH solution; aqueous potassium peroxo disulfate solution / Erwaermen des nach Ansaeuern geloesten Reaktionsprodukts mit wss. Salzsaeure
View Scheme
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
methanol; potassium hydroxide
参考文献
Baker; Savage
Journal of the Chemical Society, 1938 , p. 1602,1605
反应条件
ammonium cerium(IV) nitrate in acetonitrile
0.0833333 h;
参考文献
Venuti, Michael C.; Loe, Brad E.; Jones, Gordon H.; Young, John M.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 11 p. 2132 - 2136
