反应条件
1: NaBH4 / methanol / -20 - -10 °C 2: 71 percent / t-BuOCl, L-(+)-diisopropyl tartrate, Ti(OiPr)4 / CH2Cl2 / -20 °C 3: 0.5N NaOH / 2-methyl-propan-2-ol / Heating 4: d-10-Camphersulfonic acid / CH2Cl2 / Ambient temperature 5: m-chloroperoxybenzoic acid / CH2Cl2 / -78 °C 6: NaOAc / Heating 7: LiAlH4 View Scheme
参考文献
Ko, Soo Y.; Lee, Albert W. M.; Masamune, Satoru; Reed III, Lawrence A.; Sharpless, K. Barry; Walker, Frederick J.
Tetrahedron, 1990 , vol. 46, # 1 p. 245 - 264
