反应条件
1: PCl5 / CH2Cl2 / 2 h / 20 °C 2: acetic acid; Zn / 0.5 h / Heating 3: BH3*THF / tetrahydrofuran / 0.5 h / Heating 4: 98 percent / triethylamine / CH2Cl2 / 1 h / 20 °C 5: 82 percent / hydrochloric acid; SnCl2 / ethanol / 2 h / Heating 6: triethylamine / CH2Cl2 / 1 h / 20 °C 7: NaOH / ethanol; H2O / 2 h / 50 °C View Scheme
参考文献
Cordero-Vargas, Alejandro; Quiclet-Sire, Beatrice; Zard, Samir Z.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 18 p. 6165 - 6173