(2E)-N-烯丙基-3-苯基-2-丙烯-1-胺合成路线 （共 5 条）
反应条件
in tetrahydrofuran; methanol; chloroform; water; ethyl acetate
参考文献
Bristol-Myers Squibb Company
Patent: US6586446 B1, 2003 ;
US 6586446 B1
反应条件
2-mercapto benzoic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
T=20°C; 1 h;
参考文献
Lemarie-Audoire, Sandrine; Savignac, Monique; Dupuis, Christophe; Genet, Jean Pierre
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 1157 - 1166
反应条件
titanium(IV) isopropylate; CaH2; zinc dibromide in tetrahydrofuran
T=40°C; 12 h;
参考文献
Aida, Toshio; Kuboki, Norikatsu; Kato, Kenji; Uchikawa, Wataru; Matsuno, Chikashi; Okamoto, Sentaro
Tetrahedron Letters, 2005 , vol. 46, # 10 p. 1667 - 1669
反应条件
hydrogenchloride; triethylamine in tetrahydrofuran; water
参考文献
BASF Aktiengesellschaft
Patent: US5473080 A1, 1995 ;
反应条件
1: 90 percent / sodium hydrogencarbonate, sodium iodide / tetrahydrofuran; dimethylsulfoxide / Heating
2: 79 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / 1 h / 20 °C
View Scheme
参考文献
Lemarie-Audoire, Sandrine; Savignac, Monique; Dupuis, Christophe; Genet, Jean Pierre
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 1157 - 1166
