4-溴-3,5-二甲基苯甲酰胺合成路线 （共 5 条）
反应条件
1,3-bis-(diphenylphosphino)propane; 1,1,1,3,3,3-hexamethyl-disilazane; palladium dichloride in methanol T=80°C; 4.167 h;
参考文献
Breslin, Henry J.; Cai, Chaozhong; He, Wei; Kavash, Robert W.
Patent: US2005/203143 A1, 2005 ;
Location in patent: Page/Page column 45 ;
US 20050203143 A1
反应条件
ammonia in dichloromethane; water T=50°C; 2 h; Product distribution / selectivity;
参考文献
US2006/211861 A1, ;
Page/Page column 26 ;
US 20060211861 A1
反应条件
thionyl chloride Behandeln des erhaltenen Saeurechlorids mit wss. Ammoniak;
参考文献
Journal of the American Chemical Society, , vol. 62, p. 2995,3001
反应条件
1: With 1,3-bis-(diphenylphosphino)propane; palladium dichloride T=80°C; 4.08333 h; 2: With methanol 0.166667 h; Product distribution / selectivity;
参考文献
US2006/211861 A1, ;
Page/Page column 26-27 ;
US 20060211861 A1
反应条件
phosphorus pentachloride
参考文献
Spitzer; Wheland
Journal of the American Chemical Society, 1940 , vol. 62, p. 2995,3001
