三丁基(2-甲氧基苯基)锡合成路线 （共 23 条）
反应条件
(tBuCN)2CuOTf; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in ethyl acetate T=25°C; 12 h; Inert atmosphereGlovebox;
参考文献
Journal of the American Chemical Society, , vol. 135, # 12 p. 4648 - 4651
反应条件
triphenyl-arsane; lithium chloride; tris-(dibenzylideneacetone)dipalladium(0) in various solvent(s) T=80°C; 70 h;
参考文献
Farina, Vittorio; Krishnan, Bala; Marshall, Daniel R.; Roth, Gregory P.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5434 - 5444
反应条件
palladium diacetate; copper dichloride in tetrahydrofuran T=23°C; 0.116667 h;
参考文献
Parrish, Jay P.; Flanders, Vincent L.; Floyd, Ryan J.; Jung, Kyung Woon
Tetrahedron Letters, 2001 , vol. 42, # 44 p. 7729 - 7731
反应条件
copper(II) nitrate in tetrahydrofuran T=23°C; 2 h;
参考文献
Ghosal, Saswati; Luke, George P.; Kyler, Keith S.
Journal of Organic Chemistry, 1987 , vol. 52, # 19 p. 4296 - 4298
反应条件
in 1,2-dichloro-benzene T=180°C; 16 h; Inert atmosphere;
参考文献
Lo Fiego, Marcos J.; Lockhart, Maria T.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 22 p. 3674 - 3678
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=90°C; Stille coupling; 0.5 h; Sonication;
参考文献
Domini, Claudia E.; Silbestri, Gustavo F.; Fernandez Band, Beatriz; Chopa, Alicia B.
Ultrasonics Sonochemistry, 2012 , vol. 19, # 3 p. 410 - 414
反应条件
bis-triphenylphosphine-palladium(II) chloride in toluene T=90°C; Stille Cross Coupling; 0.5 h; Inert atmosphere;
参考文献
Luong, Martin; Domini, Claudia E.; Silbestri, Gustavo F.; Chopa, Alicia B.
Journal of Organometallic Chemistry, 2013 , vol. 723, p. 43 - 48
反应条件
aluminium trichloride in dichloromethane T=-78°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Niestroj, Michael; Neumann, Wilhelm P.
Chemische Berichte, 1996 , vol. 129, # 1 p. 45 - 51
反应条件
in tetrahydrofuran byproducts: o-anisylboronic acid; to srirred soln. of Sn-compound in THF was added soln. of BH3 in THF under N2, mixt. was left at room temp. for 1 h, refluxed for 1 h, cooled, Et2O and water was added; dried with MgSO4, solvent was removed under vac., column chromy. on silica gel with hexane and hexane-Et2O, recrystd. from water;
参考文献
Faraoni; Koll; Mandolesi; Zuniga; Podesta
Journal of Organometallic Chemistry, 2000 , vol. 613, # 2 p. 236 - 238
反应条件
borane; water in tetrahydrofuran 1 h; Heating;
参考文献
Faraoni; Koll; Mandolesi; Zuniga; Podesta
Journal of Organometallic Chemistry, 2000 , vol. 613, # 2 p. 236 - 238
