三丁基(2-甲氧基苯基)锡合成路线 （共 23 条）
反应条件
2,6-di-tert-butyl-4-methyl-phenol; triphenylphosphine; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; copper(I) bromide in N,N-dimethyl-formamide Heating;
参考文献
Saa, Jose M.; Martorell, Gabriel
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1963 - 1966
反应条件
2,6-di-tert-butyl-4-methyl-phenol; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; copper(I) bromide in N,N-dimethyl-formamide Heating;
参考文献
Saa, Jose M.; Martorell, Gabriel
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1963 - 1966
反应条件
indium T=80°C; 3 h; Inert atmosphere;
参考文献
Lo Fiego, Marcos J.; Silbestri, Gustavo F.; Chopa, Alicia B.; Lockhart, Maria T.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1707 - 1714
反应条件
magnesium in diethyl ether
refluxed overnight;; diluted with hight petroleum; ppt. washed with light petroleum; organic extracts washed with sulfuric acid, saturated hydrogencarbonate and brine; dried (Na2SO4); solvent removed; distd.; elem. anal.;;
参考文献
Kozyrod, Robert P.; Morgan, Jacqueline; Pinhey, John T.
Australian Journal of Chemistry, 1985 , vol. 38, p. 1147 - 1154
反应条件
magnesium; ethylene dibromide in tetrahydrofuran
T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere; regioselective reaction;
参考文献
Gerbino, Dario C.; Fidelibus, Pablo M.; Mandolesi, Sandra D.; Ocampo, Romina A.; Scoccia, Jimena; Podesta, Julio C.
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 24 - 32
反应条件
in 1,2-dichloro-benzene
T=180°C; 4 h; Inert atmosphere;
参考文献
Lo Fiego, Marcos J.; Silbestri, Gustavo F.; Chopa, Alicia B.; Lockhart, Maria T.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1707 - 1714
反应条件
in dichloromethane
24 h; Heating;
参考文献
Cooper, Mark S.; Heaney Harry
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5011 - 5014
反应条件
2,6-di-tert-butyl-4-methyl-phenol; triphenylphosphine; lithium chloride; bis-triphenylphosphine-palladium(II) chloride; copper(I) bromide in N,N-dimethyl-formamide
Heating;
参考文献
Saa, Jose M.; Martorell, Gabriel
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1963 - 1966
反应条件
Pd/Fe3O4; cesium fluoride in 1,4-dioxane
T=100°C; Stille Cross Coupling; 18 h;
参考文献
Prasad, Aviraboina Siva; Satyanarayana, Bollikonda
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 8 p. 2789 - 2792
反应条件
in dichloromethane
15 h; Heating;
参考文献
Cooper, Mark S.; Heaney Harry
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5011 - 5014
