3-氨基-1,3,4,5-四氢-2H-1-苯并氮杂卓-2-酮合成路线 (共 17 条)
反应条件
ammonium chloride; zinc in ethanol; water 0.166667 h; Heating;
参考文献
Lin, Wenqing; Zhang, Xiaomei; He, Ze; Jin, Yi; Gong, Liuzhu; Mi, Aiqiao
Synthetic Communications, 2002 , vol. 32, # 21 p. 3279 - 3284
反应条件
triphenylphosphine in tetrahydrofuran; water
参考文献
Jacobson, Irina C.; Wexler, Ruth R.; Nakajima, Suanne; Quan, Mimi L.; Wang, Shuaige; Smallheer, Joanne M.; Qiao, Jennifer
Patent: US2002/183324 A1, 2002 ;
US 20020183324 A1
反应条件
chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane in anhydrous xylene; water
参考文献
US4575503 A1, ;
US4410520 A1, ;
US4473575 A1, ;
反应条件
ammonia in methanol; water
参考文献
Armstrong, Joseph D. III; Eng, Kan K.; Keller, Jennifer L.; Purick, Robert M.; Hartner, Frederick W. Jr.; et al.
Tetrahedron Letters, 1994 , vol. 35, # 20 p. 3239 - 3242
反应条件
1: TMSCl, NaI, I2 2: NH3 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 23 p. 2951 - 2954
反应条件
1: sodium azide; sodium iodide / N,N-dimethyl-formamide / 24 h / 20 °C 2: triphenylphosphine / tetrahydrofuran; water / 20 h / 20 - 60 °C / |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 47 p. 9474 - 9480
反应条件
1: CH3SO3H 2: TMSCl, NaI, I2 3: NH3 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 23 p. 2951 - 2954