1-(4-甲氧基苯基)-2-[(4-甲基苯基)磺酰基]-1-乙酮合成路线 (共 18 条)
反应条件
T=30°C; 5 h; Ionic liquid;
参考文献
Kumar, Anil; Muthyala, Manoj Kumar
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5368 - 5370
反应条件
silver nitrate in tetrahydrofuran; water T=20°C; 32 h; Inert atmosphere;
参考文献
Chinese Chemical Letters, , vol. 23, # 10 p. 1115 - 1118,4
反应条件
fac-Ir(ppy)3 in dichloromethane T=20°C; Inert atmosphereIrradiation;
参考文献
Jiang, Heng; Cheng, Yuanzheng; Zhang, Yan; Yu, Shouyun
European Journal of Organic Chemistry, 2013 , # 24 p. 5485 - 5492
反应条件
iodine; triethylamine in methanol T=20°C; 8 h;
参考文献
Rawat, Vikas S.; Reddy, Perla L. M.; Sreedhar, Bojja
RSC Advances, 2014 , vol. 4, # 10 p. 5165 - 5168
反应条件
1: p-toluenesulfinic acid sodium salt With hydrogenchloride in water T=20°C; 0.0333333 h; 2: 4-ethynyl-1-methoxy-benzene With 2,6-dimethylpyridine in water T=20°C; 1.33333 h; 3: p-toluenesulfinic acid sodium salt With 2,6-dimethylpyridine; hydrogenchloride in water T=20°C; 7 h;
参考文献
Handa, Sachin; Fennewald, James C.; Lipshutz, Bruce H.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3432 - 3435
Angew. Chem., 2014 , vol. 126, # 13 p. 3500 - 3503,4
反应条件
in ethanol 1.5 h; Heating;
参考文献
Swenson, Rolf E.; Sowin, Thomas J.; Zhang, Henry Q.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9182 - 9185
反应条件
lt;Ru(PPh3)3Cl2gt; in benzene T=120°C; 7 h;
参考文献
Kamigata, Nobumasa; Udodaira, Kumiko; Shimizu, Toshio
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 783 - 786
反应条件
in neat (no solvent) T=30°C; 4 h;
参考文献
Muthyala, Manoj Kumar; Choudhary, Sunita; Kumar, Anil
RSC Advances, 2014 , vol. 4, # 27 p. 14297 - 14303
反应条件
1: 50 percent / Et3N / dimethylformamide / 48 h / Heating 2: 69 percent / <RuCl2(PPh3)3> / benzene / 7 h / 120 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 783 - 786
反应条件
1: iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide; acetonitrile / 0.5 h / 20 °C 2: dimethyl sulfoxide; acetonitrile / 1 h / 20 °C View Scheme
参考文献
Synthesis (Germany), , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699