1-(4-甲氧基苯基)-2-[(4-甲基苯基)磺酰基]-1-乙酮合成路线 （共 18 条）
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C 2: toluene-4-sulfonic acid / benzene / |Dean-Stark 3: dihydrogen peroxide / acetic acid / |Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, , vol. 50, # 2 p. 303 - 304,2
反应条件
1: toluene-4-sulfonic acid / benzene / |Dean-Stark 2: dihydrogen peroxide / acetic acid / |Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, , vol. 50, # 2 p. 303 - 304,2
反应条件
1: potassium hydroxide / ethanol / 1 h / 20 °C 2: toluene-4-sulfonic acid / benzene / |Dean-Stark 3: dihydrogen peroxide / acetic acid / |Heating View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 2 p. 296 - 297
Zhurnal Organicheskoi Khimii, , vol. 50, # 2 p. 303 - 304,2
反应条件
in dimethyl sulfoxide; acetonitrile T=20°C; 1 h;
参考文献
Samakkanad, Natthapol; Katrun, Praewpan; Techajaroonjit, Thanachart; Hlekhlai, Sornsiri; Pohmakotr, Manat; Reutrakul, Vichai; Jaipetch, Thaworn; Soorukram, Darunee; Kuhakarn, Chutima
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N0148-OP, p. 1693 - 1699
反应条件
1: acetone / 48 h / 30 °C 2: 5 h / 30 °C / Ionic liquid View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 41 p. 5368 - 5370
反应条件
in diethyl ether; dichloromethane Yield given. Yields of byproduct given;
参考文献
Schank, Kurt; Werner, Frank
Liebigs Annalen der Chemie, 1980 , # 10 p. 1477 - 1481
反应条件
acetic acid
T=20°C; 5 h; Inert atmosphere;
参考文献
Chang, Meng-Yang; Chan, Chieh-Kai; Chen, Yi-Chia
Heterocycles, 2014 , vol. 89, # 5 p. 1229 - 1236
反应条件
1: TsN3, Et3N / ethanol
2: aq. HClO4, Cu
View Scheme
参考文献
Ferdinand,G. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 1713 - 1726
