反应条件
1: 79.5 percent / Jones reagent / acetone / 1 h
2: 92.5 percent / sodium methoxide / benzene / 13 h / Ambient temperature
3: 1.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone, 2.) conc aq. HCl / 1.) benzene, room temperature, 30 min, 2.) 22 h
4: 74 percent / anhydrous potassium carbonate / dimethylformamide / 2.5 h
5: 98 percent / toluene / 0.75 h
6: 49 percent / 10percent aq. HCl / diethyl ether / 25 h
View Scheme
参考文献
Marshall, James A.; Conrow, Raymond E.
Journal of the American Chemical Society, 1980 , vol. 102, # 12 p. 4274 - 4275