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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
86553-37-9
合成路线
（共 13 条）
129748-56-7
→
反应条件
86553-37-9
反应条件
diMe-Imd-BH3; (1,3-diisopropyl-1H-imidazol-3-ium-2-yl)(phenylthio)dihydroborate in benzene-d6 T=60°C; 4 h; Irradiation;
参考文献
Pan, Xiangcheng; Lalevee, Jacques; Lacote, Emmanuel; Curran, Dennis P.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3522 - 3526
594858-64-7
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反应条件
86553-37-9
反应条件
1: With 1-n-butyl-3-methylimidazolium hexafluorophosphate in dichloromethane T=40°C; 1.5 h; Inert atmosphere; 2: With hydrogen in isopropyl alcohol T=20°C; P=760.051 Torr; 24 h; Inert atmosphere;
参考文献
Lee, Sujin; Shin, Ju Yeon; Lee, Sang-Gi
Chemistry - An Asian Journal, 2013 , vol. 8, # 9 p. 1990 - 1993
86553-34-6
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反应条件
86553-37-9
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; sodium iodide in ethylene glycol dimethyl ether T=80°C; Heating;
参考文献
Ueno, Yoshio; Tanaka, Chie; Okawara, Makoto
Chemistry Letters, 1983 , p. 795 - 796
160750-61-8
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反应条件
86553-37-9
反应条件
palladium 10 on activated carbon; hydrogen in methanol P=1500.15 Torr;
参考文献
Verendel, J. Johan; Li, Jia-Qi; Quan, Xu; Peters, Byron; Zhou, Taigang; Gautun, Odd R.; Govender, Thavendran; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 21 p. 6507 - 6513
869275-29-6
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反应条件
86553-37-9
反应条件
1: With 1H-imidazole; iodine; triphenylphosphine in acetonitrile T=0 - 20°C; Inert atmosphere; 2: With [iridium(III)(2-phenylpyridine)3]; N-ethyl-N,N-diisopropylamine in methanol; acetonitrile 0.3 h; Inert atmosphereIrradiationFlow reactor;
参考文献
Nguyen, John D.; Reiss, Barbara; Dai, Chunhui; Stephenson, Corey R. J.
Chemical Communications, 2013 , vol. 49, # 39 p. 4352 - 4354
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反应条件
86553-37-9
+
86553-38-0
反应条件
(1,2,3,4,5-pentamethyl-cyclopenta-2,4-dienylmethyl)PPh2; nickel dichloride in diethyl ether T=25°C; 3 h;
参考文献
Uemura, Minoru; Yorimitsu, Hideki; Oshima, Koichiro
Chemical Communications, 2006 , # 45 p. 4726 - 4728
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反应条件
863418-78-4
+
86553-37-9
+
1353557-81-9
反应条件
[FeCl2(3,5-tBu2-SciOPP)]; magnesium bromide in tetrahydrofuran T=0°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Hashimoto, Toru; Hatakeyama, Takuji; Nakamura, Masaharu
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1168 - 1173
50487-71-3
N-烯丙基对甲苯磺酰胺
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反应条件
86553-37-9
反应条件
1: 82 percent / KOH, tetrabutylammonium bromide / tetrahydrofuran / 15 h / Ambient temperature 2: 78 percent / Bu3SnH, AIBN / benzene / 2 h / Heating View Scheme
参考文献
Rai, K. M. Lokanatha; Hassner, Alfred
Heterocycles, 1990 , vol. 30, # 2 p. 817 - 830
129748-56-7
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反应条件
86553-37-9
+
1421130-50-8
反应条件
perdeuterated formic acid; [Au2(μ-bis(diphenylphosphanyl)methane)2][Cl]2; N-ethyl-N,N-diisopropylamine in acetonitrile T=25°C; 16 h; Inert atmosphereUV-irradiation; Overall yield = 60 percent;
参考文献
Revol, Guillaume; McCallum, Terry; Morin, Mathieu; Gagosz, Fabien; Barriault, Louis
Angewandte Chemie - International Edition, 2013 , vol. 52, # 50 p. 13342 - 13345
Angew. Chem., 2013 , vol. 125, # 50 p. 13584 - 13587,4
1303528-91-7
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反应条件
86553-37-9
反应条件
1: sodium iodide / N,N-dimethyl-formamide / 16 h / 80 °C 2: diMe-Imd-BH3; 2,2'-azo-bisisobutyronitrile / benzene / 2 h / Reflux View Scheme
参考文献
Ueng, Shau-Hua; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max; Curran, Dennis P.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3415 - 3420
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