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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
86553-38-0
合成路线
（共 9 条）
5368-63-8
+
70-55-3
对甲苯磺酰胺
→
反应条件
86553-38-0
反应条件
trifluorormethanesulfonic acid in toluene T=120°C; 35 h;
参考文献
Shi, Wei; Bai, Chun-Mei; Zhu, Kai; Cui, Dong-Mei; Zhang, Chen
Tetrahedron, 2014 , vol. 70, # 2 p. 434 - 438
→
反应条件
86553-38-0
反应条件
1,3-bis(diphenylphosphino)ethane; cobalt(II) chloride in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Ohmiya, Hirohisa; Wakabayashi, Katsuyu; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2006 , vol. 62, # 10 p. 2207 - 2213
86553-35-7
→
反应条件
86553-38-0
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; sodium iodide in ethylene glycol dimethyl ether T=80°C; 1 h; Heating;
参考文献
Ueno, Yoshio; Tanaka, Chie; Okawara, Makoto
Chemistry Letters, 1983 , p. 795 - 796
1392282-82-4
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反应条件
86553-38-0
反应条件
palladium 10 on activated carbon; hydrogen in methanol P=1500.15 Torr;
参考文献
Verendel, J. Johan; Li, Jia-Qi; Quan, Xu; Peters, Byron; Zhou, Taigang; Gautun, Odd R.; Govender, Thavendran; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 21 p. 6507 - 6513
→
反应条件
86553-37-9
+
86553-38-0
反应条件
(1,2,3,4,5-pentamethyl-cyclopenta-2,4-dienylmethyl)PPh2; nickel dichloride in diethyl ether T=25°C; 3 h;
参考文献
Uemura, Minoru; Yorimitsu, Hideki; Oshima, Koichiro
Chemical Communications, 2006 , # 45 p. 4726 - 4728
32121-04-3
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反应条件
86553-38-0
反应条件
1: potassium carbonate / acetonitrile / 24 h / 60 °C 2: sodium iodide / acetone / 7 h / |Reflux 3: nickel dichloride; bis(cyclopentadienyl)titanium dichloride; tri-cyclo-hexyl-phosphine; manganese; water / tetrahydrofuran / 20 °C / |Inert atmosphere View Scheme
参考文献
Millan, Alba; Alvarez De Cienfuegos, Luis; Miguel, Delia; Campana, Araceli G.; Cuerva, Juan M.
Organic Letters, 2012 , vol. 14, # 23 p. 5984 - 5987
1392283-20-3
→
反应条件
86553-38-0
反应条件
1: Grubb's 2nd generation catalyst / dichloromethane 2: palladium 10 on activated carbon; hydrogen / methanol / 1500.15 Torr View Scheme
参考文献
Verendel, J. Johan; Li, Jia-Qi; Quan, Xu; Peters, Byron; Zhou, Taigang; Gautun, Odd R.; Govender, Thavendran; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 21 p. 6507 - 6513
50487-71-3
N-烯丙基对甲苯磺酰胺
→
反应条件
86553-38-0
反应条件
1: potassium carbonate / acetonitrile / Inert atmosphere 2: Grubb's 2nd generation catalyst / dichloromethane 3: palladium 10 on activated carbon; hydrogen / methanol / 1500.15 Torr View Scheme
参考文献
Verendel, J. Johan; Li, Jia-Qi; Quan, Xu; Peters, Byron; Zhou, Taigang; Gautun, Odd R.; Govender, Thavendran; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 21 p. 6507 - 6513
437709-07-4
→
反应条件
86553-38-0
反应条件
1: potassium carbonate / acetonitrile / Inert atmosphere 2: Grubb's 2nd generation catalyst / dichloromethane 3: palladium 10 on activated carbon; hydrogen / methanol / 1500.15 Torr View Scheme
参考文献
Verendel, J. Johan; Li, Jia-Qi; Quan, Xu; Peters, Byron; Zhou, Taigang; Gautun, Odd R.; Govender, Thavendran; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 21 p. 6507 - 6513
