sulfur; sodium hydrogencarbonate in tetrahydrofuran; water
T=35°C; Gewald reaction; 1.5 h;
参考文献
Barnes, David M.; Haight, Anthony R.; Hameury, Thomas; McLaughlin, Maureen A.; Mei, Jianzhang; Tedrow, Jason S.; Riva Toma, Joan Dalla
Tetrahedron, 2006 , vol. 62, # 49 p. 11311 - 11319
1: 86 percent / 1,1,1,3,3,3-hexamethyldisilazane; acetic acid / 65 °C
2: 73 percent / S8; NaHCO3 / tetrahydrofuran; H2O / 1.5 h / 35 °C
View Scheme
参考文献
Barnes, David M.; Haight, Anthony R.; Hameury, Thomas; McLaughlin, Maureen A.; Mei, Jianzhang; Tedrow, Jason S.; Riva Toma, Joan Dalla
Tetrahedron, 2006 , vol. 62, # 49 p. 11311 - 11319
