2-(1,3-二氧戊环-2-基)乙基三苯基溴化磷合成路线 （共 3 条）
反应条件
in acetonitrile 24 h;
参考文献
Dirat, Olivier; Kouklovsky, Cyrille; Langlois, Yves
Journal of Organic Chemistry, 1998 , vol. 63, # 19 p. 6634 - 6642
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 90 percent / tetrahydrofuran / 1 h / 0 °C 2.1: H2 / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr 3.1: 99 percent / PPTS / acetone; H2O / 12 h / Heating 4.1: 56 percent / tetrahydrofuran / 1 h / -40 °C 5.1: 88 percent / Dess-Martin periodinane / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Ohno, Hiroaki; Okumura, Mitsuaki; Maeda, Shin-Ichiro; Iwasaki, Hiroki; Wakayama, Ryutaro; Tanaka, Tetsuaki
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7722 - 7732
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 0 °C 1.2: 90 percent / tetrahydrofuran / 1 h / 0 °C 2.1: H2 / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr 3.1: 99 percent / PPTS / acetone; H2O / 12 h / Heating View Scheme
参考文献
Ohno, Hiroaki; Okumura, Mitsuaki; Maeda, Shin-Ichiro; Iwasaki, Hiroki; Wakayama, Ryutaro; Tanaka, Tetsuaki
Journal of Organic Chemistry, 2003 , vol. 68, # 20 p. 7722 - 7732
