ammonium hydroxide; nickel in ethanol 1.5 h; Heating;

ammonia in methanol T=130°C; 8 h; high pressure;

1: 78 percent / ammonia / methanol / 10 h / 135 °C 2: 68 percent / aq. ammonia / Raney Ni / ethanol / 1.5 h / Heating View Scheme

1: 80 percent / ammonia / methanol / 20 h / Ambient temperature 2: 78 percent / ammonia / methanol / 10 h / 135 °C 3: 68 percent / aq. ammonia / Raney Ni / ethanol / 1.5 h / Heating View Scheme

1: 61.5 percent / sodium hydride / dimethylformamide / 1 h / Ambient temperature 2: 80 percent / ammonia / methanol / 20 h / Ambient temperature 3: 78 percent / ammonia / methanol / 10 h / 135 °C 4: 68 percent / aq. ammonia / Raney Ni / ethanol / 1.5 h / Heating View Scheme

1: 37 percent / 60percent NaH / dimethylformamide / 0.5 h / Ambient temperature 2: 47 percent / NH3 / methanol / 8 h / 130 °C / high pressure View Scheme

phosphoric acid trimethyl ester; ammonium hydroxide; trichlorophosphate T=0 - 5°C; 1.5 h;