N-[2-甲基-3-(4-吗啉基)丙基]-3-苯基-1,2-恶唑-5-胺合成路线 （共 3 条）
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride in benzene
12 h; Ambient temperature;
参考文献
Tatee; Kurashige; Shiozawa; Narita; Takei; Ito; Miyazaki; Yamanaka; Mizugaki; Sakamoto
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1634 - 1642
反应条件
1: 72 percent / pyridine / CHCl3 / 2 h / -5 °C
2: 84 percent / ethanol / 8 h / Heating
3: 89 percent / 70percent sodium bis-(2-methoxyethoxy)aluminum hydride in toluene / benzene / 12 h / Ambient temperature
View Scheme
参考文献
Tatee; Kurashige; Shiozawa; Narita; Takei; Ito; Miyazaki; Yamanaka; Mizugaki; Sakamoto
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1634 - 1642
反应条件
1: 84 percent / ethanol / 8 h / Heating
2: 89 percent / 70percent sodium bis-(2-methoxyethoxy)aluminum hydride in toluene / benzene / 12 h / Ambient temperature
View Scheme
参考文献
Tatee; Kurashige; Shiozawa; Narita; Takei; Ito; Miyazaki; Yamanaka; Mizugaki; Sakamoto
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1634 - 1642
