反应条件
1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in ethylene glycol dimethyl ether T=0°C; Metallation; 0.25 h; 2: α,α,α-trifluoro-m-tolualdehyde in ethylene glycol dimethyl ether T=0°C; Condensation; 0.25 h;
参考文献
Liu, Yongxiang; Li, Xiben; Lin, Guang; Xiang, Zheng; Xiang, Jing; Zhao, Mingzhe; Chen, Jiahua; Yang, Zhen
Journal of Organic Chemistry, 2008 , vol. 73, # 12 p. 4625 - 4629
