1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
1: With sodium hydride in tetrahydrofuran T=20°C; Horner-Wadsworth-Emmons reaction; 2: With 3-chloro-benzenecarboperoxoic acid in chloroform T=20°C; 3: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C;
1: With potassium carbonate Horner-Wadsworth-Emmons olefination; 6 h; Neat (no solvent)high-speed ball milling; 2: With Oxonereg; 12 h; Neat (no solvent)high-speed ball milling; optical yield given as percent dediastereoselective reaction;
参考文献
Shearouse, William C.; Korte, Chelsea M.; Mack, James
Green Chemistry, 2011 , vol. 13, # 3 p. 598 - 601
