1: diethoxyphosphoryl-acetic acid ethyl ester With potassium tert-butylate in 1,4-dioxane
T=20°C; 0.666667 h;
2: cyclohexenon in 1,4-dioxane
6 h; Heating; Further stages. Title compound not separated from byproducts.;
参考文献
Doering; Ekmanis; Belfield; Klaerner; Krawczyk
Journal of the American Chemical Society, 2001 , vol. 123, # 23 p. 5532 - 5541
1: With sodium hydride in tetrahydrofuran
T=20°C; Horner-Wadsworth-Emmons reaction;
2: With 3-chloro-benzenecarboperoxoic acid in chloroform
T=20°C;
3: With lithium aluminium tetrahydride in tetrahydrofuran
T=20°C;
