9,10-双(2-萘基)蒽-2-硼酸合成路线 （共 3 条）
反应条件
1: 2-bromo-9,10-di(naphthalene-2-yl)anthracene With n-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: boric acid trimethyl ester in tetrahydrofuran T=-78 - 20°C; 1 h; 3: With hydrogenchloride; water in tetrahydrofuran
参考文献
Samsung SDI Co., Ltd.
Patent: EP1970376 A1, 2008 ;
Location in patent: Page/Page column 12-13 ;
反应条件
1: 2-bromo-9,10-di(naphthalene-2-yl)anthracene With n-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: tri-isopropoxy-borane in tetrahydrofuran T=20°C; 3: With hydrogenchloride in tetrahydrofuran; water T=0°C;
参考文献
Samsung Mobile Display Co., Ltd.
Patent: EP2292604 A2, 2011 ;
Location in patent: Page/Page column 24-25 ;
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=-78 - 20°C; 3 h; 3: With hydrogenchloride in tetrahydrofuran; hexane; water 1 h;
参考文献
IDEMITSU KOSAN CO., LTD.
Patent: EP1734038 A1, 2006 ;
Location in patent: Page/Page column 44 ;
