2,5-DIMETHOXYPYRIDINE合成路线 (共 3 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=50°C; 3 h;
参考文献
Mahiout, Zahia; Lomberget, Thierry; Goncalves, Sylvie; Barret, Roland
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 8 p. 1364 - 1376
反应条件
1: 2,5-dimethoxypyridine With methyllithium; diisopropylamine in tetrahydrofuran; diethyl ether
T=-40 - 0°C;
2: 1-piperidinecarboxaldehyde in tetrahydrofuran; diethyl ether
T=-40°C; 2 h;
参考文献
Mahiout, Zahia; Lomberget, Thierry; Goncalves, Sylvie; Barret, Roland
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 8 p. 1364 - 1376
反应条件
1: 2,5-dimethoxypyridine With methyllithium; diisopropylamine in tetrahydrofuran; diethyl ether
T=-40 - 0°C;
2: 1-piperidinecarboxaldehyde in tetrahydrofuran; diethyl ether
T=-40°C; 2 h;
参考文献
Mahiout, Zahia; Lomberget, Thierry; Goncalves, Sylvie; Barret, Roland
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 8 p. 1364 - 1376