(5-氰基-2-甲基苯基)硼酸合成路线 (共 1 条)
反应条件
1: 3-bromo-4-methyl-benzonitrile With n-butyllithium in tetrahydrofuran; hexane
T=-98°C;
2: With hydrogenchloride in diethyl ether
3: boric acid trimethyl ester in tetrahydrofuran; hexane
T=-98 - 20°C; 0.5 h; Further stages.;
参考文献
Zhong, Zhenlin; Anslyn, Eric V.
Journal of the American Chemical Society, 2002 , vol. 124, # 31 p. 9014 - 9015