(E)-N-[4-(2,8-二氯-10,11-二氢二苯并[b,f]硫杂卓-10-基)-1-哌嗪基]-1-苯基甲亚胺合成路线 （共 6 条）
反应条件
in ethanol
0.25 h; Heating;
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 99 percent / CaCl2, HCl(g) / benzene / 5 h / Ambient temperature
2: 83 percent / 6 h / 110 °C
3: 80 percent / 85percent KOH / ethanol / 3 h / Heating
4: 72 percent / NaNO2, aq. HCl
5: 88 percent Turnov. / LiAlH4 / diethyl ether
6: 70 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 72 percent / NaNO2, aq. HCl
2: 88 percent Turnov. / LiAlH4 / diethyl ether
3: 70 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 88 percent Turnov. / LiAlH4 / diethyl ether
2: 70 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 80 percent / 85percent KOH / ethanol / 3 h / Heating
2: 72 percent / NaNO2, aq. HCl
3: 88 percent Turnov. / LiAlH4 / diethyl ether
4: 70 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 83 percent / 6 h / 110 °C
2: 80 percent / 85percent KOH / ethanol / 3 h / Heating
3: 72 percent / NaNO2, aq. HCl
4: 88 percent Turnov. / LiAlH4 / diethyl ether
5: 70 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
