(E)-N-[4-(2-氯-10,11-二氢二苯并[b,f]硫杂卓-10-基)-1-哌嗪基]-1-(3,4-二甲氧基苯基)甲亚胺合成路线 （共 3 条）
反应条件
in ethanol
0.25 h; Heating;
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 97 percent / LiAlH4 / diethyl ether / 5 h / Ambient temperature
2: 84 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
反应条件
1: 76 percent / NaNO2, aq. HCl / 1.) 75-80 deg C, 3 h, 2.) R.T., overnight.
2: 97 percent / LiAlH4 / diethyl ether / 5 h / Ambient temperature
3: 84 percent / ethanol / 0.25 h / Heating
View Scheme
参考文献
Bartl; Holubek; Svatek; et al.
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 4 p. 1173 - 1186
