1-氨基-3,6,9-三噁-11-十一醇合成路线 （共 14 条）
反应条件
water; triphenylphosphine in tetrahydrofuran 4 h; Ambient temperature;
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2009/132310 A1, 2009 ;
Location in patent: Page/Page column 66 ;
反应条件
hydrazine in methanol T=20 - 50°C;
参考文献
WO2009/108484 A1, ;
Page/Page column 24; 25 ;
反应条件
1: 33 percent / triethylamine / CH2Cl2 / 2 h / 0 °C 2: 89 percent / sodium azide / acetonitrile / 36 h / Heating 3: 86 percent / triphenylphosphine; water / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 5 p. 1120 - 1121
反应条件
1: 89 percent / sodium azide / acetonitrile / 36 h / Heating 2: 86 percent / triphenylphosphine; water / tetrahydrofuran / 4 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 5 p. 1120 - 1121
反应条件
1: 1-azido-11-hydroxy-3,6,9-trioxaundecane With triphenylphosphine in tetrahydrofuran T=0 - 20°C; 12 h; 2: water 12 h;
参考文献
Aleman Garcia, Miguel A.; Bampos, Nick
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 1 p. 27 - 30
反应条件
triphenylphosphine in tetrahydrofuran; pyridine; water
反应条件
trifluoroacetic acid in dichloromethane T=20°C;
参考文献
Palanki, Moorthy S.S.; Bhat, Abhijit; Bolanos, Ben; Brunel, Florence; Del Rosario, Joselyn; Dettling, Danielle; Horn, Mark; Lappe, Rodney; Preston, Ryan; Sievers, Annette; Stankovic, Nebojsa; Woodnut, Gary; Chen, Gang
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 2 p. 402 - 406
反应条件
1.1: 94 percent / sodium azide / dimethylformamide / 2.5 h / 110 °C 2.1: Ph3P / tetrahydrofuran / 10 h / 20 °C 2.2: 99 percent / H2O / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 13 p. 4494 - 4503
参考文献
Gartiser, Thierry; Selve, Claude; Mansuy, Laurence; Robert, Alain; Delpuech, Jean-Jacques
Journal of Chemical Research, Miniprint, 1984 , # 9 p. 2672 - 2691
反应条件
1: 96 percent / PPh3 / CCl4 / 24 h / Heating 2: 98 percent / NaN3 3: 94 percent / H2 / Pd View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 2672 - 2691
