反应条件
1: 93.5 percent / NaIO4 / methanol; H2O / 48 h / Ambient temperature
2: 190 mg / LDA / tetrahydrofuran / 1.) 3 h, -78 deg C, 2.) 2 h, 0 deg C, 3.) 17 h, r.t.
3: Al-Hg / tetrahydrofuran; H2O / 4 h / Heating
View Scheme
参考文献
Ohtsuka, Yasuo; Oishi, Takeshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 2 p. 443 - 453
