in hexadeuterioacetone to cold (-78 °C) soln. of Ti complex in acetone-d6 added soln. of HgCl2 in acetone-d6 under N2; warmed to room temp., monitored by NMR;

hydrogenchloride in diethyl ether byproducts: C6H5Cl, CH4; to cold (-78 °C) soln. of Ti complex in Et2O added dropwise withstirring soln. of anhyd. HCl in Et2O under N2; warmed to room temp., evapd., monitored by NMR;

hydrogenchloride in diethyl ether byproducts: C6H5Cl, CH4; to cold (-78 °C) soln. of Ti complex in Et2O added dropwise withstirring soln. of anhyd. HCl in Et2O under N2; warmed to room temp., evapd., monitored by NMR;

in hexadeuterioacetone to cold (-78 °C) soln. of Ti complex in acetone-d6 added soln. of HgCl2 in acetone-d6 under N2; warmed to room temp., monitored by NMR;