1-CBZ-3-哌啶乙酸甲酯合成路线 (共 7 条)
反应条件
dichloro-acetic acid in acetonitrile Irradiation;
参考文献
Jeon, Yoon T.; Lee, Chao-Pin; Mariano, Patrick S.
Journal of the American Chemical Society, 1991 , vol. 113, # 23 p. 8847 - 8863
反应条件
1: 71 percent / CH2Cl2 / 78 h / Heating 2: 78 percent / DCA / acetonitrile / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 113, # 23 p. 8847 - 8863
反应条件
1: Hg(OAc)2 / 43 h / 210 °C / in a sealed tube 2: silver(I) oxide / aq. ethanol / 0.33 h 3: hydrogen / platinum oxide / methanol / 0.5 h / 760 Torr / Ambient temperature 4: 1.) KOH / 1.) EtOH, 43 h reflux; 2.) 10 h room temperature 5: 38 percent / diethyl ether / 0.67 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 4 p. 1191 - 1198
反应条件
1: silver(I) oxide / aq. ethanol / 0.33 h 2: hydrogen / platinum oxide / methanol / 0.5 h / 760 Torr / Ambient temperature 3: 1.) KOH / 1.) EtOH, 43 h reflux; 2.) 10 h room temperature 4: 38 percent / diethyl ether / 0.67 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 4 p. 1191 - 1198
反应条件
1: hydrogen / platinum oxide / methanol / 0.5 h / 760 Torr / Ambient temperature 2: 1.) KOH / 1.) EtOH, 43 h reflux; 2.) 10 h room temperature 3: 38 percent / diethyl ether / 0.67 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 4 p. 1191 - 1198
反应条件
1: 1.) KOH / 1.) EtOH, 43 h reflux; 2.) 10 h room temperature 2: 38 percent / diethyl ether / 0.67 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 4 p. 1191 - 1198
反应条件
in diethyl ether 0.666667 h;
参考文献
Imanishi; Miyashita; Nakai; et al.
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 4 p. 1191 - 1198