2-特戊酰氨基-3-(alpha-羟基苄基)吡啶合成路线 (共 5 条)
反应条件
1: MnO2 / CH2Cl2 2: aq. HCl View Scheme
参考文献
Estel; Linard; Marsais; Godard; Queguiner
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 1 p. 105 - 112
反应条件
manganese(IV) oxide in toluene 3 h; Heating;
参考文献
Estel; Linard; Marsais; Godard; Queguiner
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 1 p. 105 - 112
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; diethyl ether; hexane
1.) -10 degC, 2 h, 2.) 0 degC, 2 h;
参考文献
Estel; Linard; Marsais; Godard; Queguiner
Journal of Heterocyclic Chemistry, 1989 , vol. 26, # 1 p. 105 - 112
反应条件
1: 79 percent / triethylamine / CH2Cl2 / 2 h / Ambient temperature
2: n-BuLi / THF, hexane, 0 deg C to room temp.
View Scheme
参考文献
Turner, James A.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3401 - 3408
反应条件
1: 79 percent / triethylamine / CH2Cl2 / 2 h / Ambient temperature
2: n-BuLi / THF, hexane, 0 deg C to room temp.
View Scheme
参考文献
Turner, James A.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3401 - 3408