反应条件
1: 76 percent / 50percent NaOH / H2O / 24 h / Heating
2: 86 percent / SOCl2 / 18 h / 80 °C
3: 1.) K, 2.) Br2 / 1.) THF, 15 min, 2.) THF, 24 h, reflux
4: 60 percent / 1N HCl / diethyl ether / 2 h / Ambient temperature
View Scheme
参考文献
Gartiser, Thierry; Selve, Claude; Mansuy, Laurence; Robert, Alain; Delpuech, Jean-Jacques
Journal of Chemical Research, Miniprint, 1984 , # 9 p. 2672 - 2691
