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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
868615-35-4
合成路线
（共 10 条）
868615-50-3
→
反应条件
868615-35-4
反应条件
lead(IV) acetate; iodine in tetrachloromethane T=80°C; Kochi reaction; 1.5 h;
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
868615-47-8
→
反应条件
868615-35-4
反应条件
1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 2: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
868615-32-1
→
反应条件
868615-35-4
反应条件
1.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 1.2: 90 percent / DBU / toluene / 1 h / 110 °C 2.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 3.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 4.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
868615-31-0
→
反应条件
868615-35-4
反应条件
1.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 2.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 2.2: 90 percent / DBU / toluene / 1 h / 110 °C 3.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 4.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 5.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
7424-82-0
→
反应条件
868615-35-4
反应条件
1.1: 89 percent / CH2Cl2 / 4 h / 20 °C 2.1: 89 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C 3.1: triethylamine; DMAP / CH2Cl2 / 1.5 h / 0 - 20 °C 3.2: 90 percent / DBU / toluene / 1 h / 110 °C 4.1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 5.1: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 6.1: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
868615-33-2
→
反应条件
868615-35-4
反应条件
1: 70 percent / CuI / diethyl ether / 1 h / -30 °C 2: 75 percent / sodium hydroxide / methanol / 4 h / 20 °C 3: 65 percent / Pb(OAc)4; I2 / CCl4 / 1 h / 80 °C / Irradiation View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
918813-53-3
→
反应条件
868615-35-4
反应条件
1: 70 percent / diethyl ether / 2 h / -78 °C 2: 80 percent / aq. KOH / methanol / 12 h / 20 °C 3: 65 percent / Pb(OAc)4; I2 / CCl4 / 1.5 h / 80 °C View Scheme
参考文献
Drege, Emmanuelle; Morgant, Georges; Desmaele, Didier
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7263 - 7266
868615-46-7
→
反应条件
868615-35-4
反应条件
1: 90 percent / DBU / toluene / 1.5 h / 110 °C 2: 70 percent / diethyl ether / 2 h / -78 °C 3: 80 percent / aq. KOH / methanol / 12 h / 20 °C 4: 65 percent / Pb(OAc)4; I2 / CCl4 / 1.5 h / 80 °C View Scheme
参考文献
Drege, Emmanuelle; Morgant, Georges; Desmaele, Didier
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7263 - 7266
868615-35-4
+
127-09-3
乙酸钠
→
反应条件
918813-56-6
反应条件
in N,N-dimethyl-formamide T=110°C; 3 h;
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
868615-35-4
→
反应条件
918813-63-5
反应条件
1: 70 percent / dimethylformamide / 3 h / 110 °C 2: 80 percent / potassium carbonate / methanol / 5 h / 20 °C View Scheme
参考文献
Drege, Emmanuelle; Tominiaux, Cyrille; Morgant, Georges; Desmaele, Didier
European Journal of Organic Chemistry, 2006 , # 21 p. 4825 - 4840
