1: octa-3,7-diynyl-benzene With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 2: With tBuOOLi in tetrahydrofuran; toluene T=-78 - 0°C; 2.5 h; 3: tri-isopropylsylil trifluoromethane sulfonate in tetrahydrofuran; toluene T=-78 - 0°C;