反应条件
1: 1,1-dibromo-3,3-dimethyl-dec-5-yn-2-one With lithium hexamethyldisilazane in tetrahydrofuran; hexane
T=-78°C; 0.333333 h;
2: With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
3: tri-isopropylsylil trifluoromethane sulfonate in tetrahydrofuran; hexane
T=-78 - 0°C;
参考文献
Sun, Jianwei; Kozmin, Sergey A.
Journal of the American Chemical Society, 2005 , vol. 127, # 39 p. 13512 - 13513