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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
86901-19-1
合成路线
（共 43 条）
823-69-8
7,7-二氯二环[4.1.0]庚烷
+
86901-19-1
→
反应条件
1588-50-7
+
286-08-8
双环[4.1.0]庚烷
+
286-34-0
双环[3.1.1]庚烷
+
279-18-5
+
110079-21-5
+
110079-22-6
反应条件
in tetrahydrofuran T=-20°C; influence of halogen and reaction temperature; Product distributionMechanism;
参考文献
Bogdanovic, Borislav; Schlichte, Klaus; Westeppe, Uwe
Chemische Berichte, 1988 , vol. 121, p. 27 - 32
78-86-4
氯代仲丁烷
+
86901-19-1
→
反应条件
10394-54-4
反应条件
in diethyl ether 48 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
109-69-3
1-氯丁烷
+
86901-19-1
→
反应条件
47205-57-2
+
10394-60-2
+
126694-89-1
+
126694-90-4
反应条件
in tetrahydrofuran T=40°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
109-69-3
1-氯丁烷
+
86901-19-1
→
反应条件
47205-57-2
+
10394-60-2
+
693-04-9
氯丁基镁
+
126694-91-5
反应条件
in toluene 24 h; Ambient temperature; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
86901-19-1
+
513-36-0
氯代异丁烷
→
反应条件
126694-97-1
反应条件
in toluene 1 h; Heating; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
86901-19-1
+
513-36-0
氯代异丁烷
→
反应条件
126694-97-1
反应条件
in toluene 1 h; Heating; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
86901-19-1
+
513-36-0
氯代异丁烷
→
反应条件
126694-97-1
反应条件
in toluene 1 h; Heating; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
86901-19-1
+
563-47-3
→
反应条件
5674-01-1
+
95164-05-9
+
126695-02-1
+
126695-03-2
反应条件
in tetrahydrofuran T=-78°C; 12 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
86901-19-1
+
107-05-1
→
反应条件
120-12-7
+
84332-59-2
+
2622-05-1
+
126695-01-0
反应条件
in tetrahydrofuran T=-78°C; 12 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
507-20-0
+
86901-19-1
→
反应条件
13387-48-9
反应条件
in tetrahydrofuran T=40°C; 2 h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bogdanovic, Borislav; Janke, Nikolaus; Kinzelmann, Hans-Georg
Chemische Berichte, 1990 , vol. 123, # 7 p. 1507 - 1515
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